Luis Gerardo Zepeda Vallejo

Work

Instituto Politécnico Nacional

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Researcher/Teacher

Mexico

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Education

Instituto Politécnico Nacional

Mexico
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PhD

Centro de Investigación y de Estudios Avanzados del Instituto Politécnico Nacional

Mexico
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MSc

Universidad Michoacana de San Nicolás de Hidalgo

Mexico
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Bachelor

Publications

1H Nuclear Magnetic Resonance-Based Targeted and Untargeted Metabolomics Profiling of Retail Samples of Cuachalalate (Amphipterygium adstringens)

Molecules

journal-article

NMR-Based Metabolomic Approach to Study Growth of Phaseolus vulgaris L. Seedlings Through Leaf Application of Nanofertilizers and Biofertilizers

International Journal of Molecular Sciences

journal-article

Structural Analysis of the Michael-Michael Ring Closure (MIMIRC) Reaction Products

Molecules

journal-article

A semi-targeted NMR-based chemical profiling of retail samples of Mexican gordolobo

Journal of Pharmaceutical and Biomedical Analysis

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Changes in the metabolomic profiling of Allium cepa L. (onion) plants infected with Stemphylium vesicarium

European Journal of Plant Pathology

journal-article

Hibiscus Acid from Hibiscus sabdariffa L. Inhibits Flagellar Motility and Cell Invasion in Salmonella enterica

Molecules

journal-article

Structural and physicochemical characteristics of one-step PAMAM dendrimeric nanoparticles

Colloids and Surfaces A: Physicochemical and Engineering Aspects

journal-article

Bean cultivars (Phaseolus vulgaris L.) under the spotlight of NMR metabolomics

Food Research International

journal-article

Consistency of a dialyzable leucocyte extract manufactured at GMP facilities by nuclear magnetic resonance spectroscopy

Journal of Pharmaceutical and Biomedical Analysis

journal-article

Quality attributes of partially hydrolyzed collagen in a liquid formulation used for skin care

Journal of Cosmetic Dermatology

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1H-NMR metabolomics profiling of recombinant tobacco plants holding a promoter of a sesquiterpene cyclase

Phytochemical Analysis

journal-article

Anthraquinones: Versatile Organic Photocatalysts

ChemCatChem

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Anti-amoebic Activity of Leaf Extracts and Aporphine Alkaloids Obtained from Annona purpurea

Planta Medica

journal-article

Experimental races of Capsicum annuum cv. jalapeño: Chemical characterization and classification by 1H NMR/machine learning

Food Research International

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Extraction of alkaloids using ultrasound from pulp and by-products of soursop fruit (Annona muricata L.)

Applied Sciences (Switzerland)

journal-article

New Triazole and Isoxazole Compounds as Corrosion Inhibitors for Cu-Ni (90/10) Alloy and Galvanized Steel Substrates

Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science

journal-article

Revealing the 1H NMR metabolome of mirasol chili peppers (Capsicum annuum) infected by Candidatus Phytoplasma trifolii

Food Research International

journal-article

Study of nutritional quality of pomegranate (Punica granatum L.) juice using 1H NMR-based metabolomic approach: A comparison between conventionally and organically grown fruits

LWT

journal-article

1 H NMR-based fingerprinting of eleven Mexican Capsicum annuum cultivars

Food Research International

journal-article

1 H NMR-based metabolomics profiling of ten new races from Capsicum annuum cv. serrano produced in Mexico

Food Research International

journal-article

1H-NMR Based Metabolomics Profiling of Citrus Juices Produced in Veracruz, México

Chemistry and Biodiversity

journal-article

Determination of Peptide Profile Consistency and Safety of Collagen Hydrolysates as Quality Attributes

Journal of Food Science

journal-article

Hypolipidemic effect of trixis angustifolia aqueous extract on triton WR-1339- And high-fat diet-induced hyperlipidemic mice

Natural Product Communications

journal-article

Identity Profiling of Complex Mixtures of Peptide Products by Structural and Mass Mobility Orthogonal Analysis

Analytical Chemistry

journal-article

NMR-based metabonomic approach reveals changes in the urinary and fecal metabolome caused by resveratrol

Journal of Pharmaceutical and Biomedical Analysis

journal-article

Trixis angustifolia hexanic extract displays  synergistic antibacterial activity against M. tuberculosis

Natural Product Research

journal-article

1H NMR-based metabolomic profiling for identification of metabolites in Capsicum annuum cv. mirasol infected by beet mild curly top virus (BMCTV)

Food Research International

journal-article

Alternative use of extracts of Chipilín leaves (Crotalaria longirostrata Hook. & Arn) as antimicrobial

Sustainability (Switzerland)

journal-article

Configurational study of an aporphine alkaloid from annona purpurea

Natural Product Communications

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Antimycobacterial and hypolipemiant activities of Bidens odorata (Cavanilles)

Journal of Ethnopharmacology

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Synthesis and stereoselective evaluation of a (1R)-(–)-myrtenal-derived pseudo C2-symmetric dodecaheterocycle as a potential heterofunctional chiral auxiliary

Tetrahedron Letters

journal-article

An 1H NMR-based metabolomic approach to compare the chemical profiling of retail samples of ground roasted and instant coffees

Food Research International

journal-article

1H NMR-based metabolomic fingerprinting to determine metabolite levels in serrano peppers (Capsicum annum L.) grown in two different regions.

Food Research International

journal-article

Nucleophilic additions on acetyldioxanes derived from (−)-(1R)-myrtenal used as chiral auxiliaries: substituent effects on the stereochemical outcome

Tetrahedron Asymmetry

journal-article

1H NMR-based metabolomic fingerprinting to determine metabolite levels in serrano peppers (Capsicum annum L.) grown in two different regions

Food Research International

journal-article

Nucleophilic additions on acetyldioxanes derived from (−)-(1R)-myrtenal used as chiral auxiliaries: substituent effects on the stereochemical outcome

Tetrahedron: Asymmetry

journal-article

NMR-based metabonomic analysis of normal rat urine and faeces inresponse to (±)-venlafaxine treatment

Journal of Pharmaceutical and Biomedical Analysis

journal-article

NMR-based pharmacometabonomic analysis of normal rat urine and faeces in response to (±)-venlafaxine treatment

Journal of Pharmaceutical and Biomedical Analysis

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NMR-based metabonomic analysis of physiological responses to starvation and refeeding in the rat

Journal of Proteome Research

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NMR-Based Metabonomic Analysis of Physiological Responses to Starvation and Refeeding in the Rat

Journal of Proteome Research

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Versatile and regioselective synthesis of polysubstituted and highly oxygenated phenols via Dötz reaction of α-alkoxyvinyl(ethoxy)carbene complexes with alkynes

Journal of Organometallic Chemistry

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Functionalized α-oximinoketones as building blocks for the construction of imidazoline-based potential chiral auxiliaries

Tetrahedron Asymmetry

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Effects of Cooking Methods on Phenolic Compounds in Xoconostle (Opuntia joconostle)

Plant Foods for Human Nutrition

journal-article

Synthesis of fluorescent oligo(P-phenyleneethynylene) (OPE3) via sonogashira reactions

Journal of the Mexican Chemical Society

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Efficient synthetic approach to substituted benzo[b]furans and benzo[b]thiophenes by iodine-promoted cyclization of enaminones

Journal of Heterocyclic Chemistry

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Effects of microfluidisation process on the amounts and distribution of encapsulated and non-encapsulated α-tocopherol microcapsules obtained by spray drying

Food Research International

journal-article

Oligomerization of 10,16-dihydroxyhexadecanoic acid and methyl 10,16-dihydroxyhexadecanoate catalyzed by lipases

Molecules

journal-article

Extraction, stability, and separation of betalains from opuntia joconostle cv. using response surface methodology

Journal of Agricultural and Food Chemistry

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NMR-based conformational analysis of perezone and analogues

Magnetic Resonance in Chemistry

journal-article

Effect of thermal sterilization on ferulic, coumaric and cinnamic acids: Dimerization and antioxidant activity

Journal of the Science of Food and Agriculture

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Efficient preparation of α-ketoacetals

Molecules

journal-article

Preparation of (R)- and (S)-2-Methoxy-2-phenylpent-3-ynoic Acids and their Use as Reliable Chiral Derivatizing Agents

The Journal of Organic Chemistry

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Diastereoselective preparation of (R)- and (S)-2-methoxy-2-phenylpent-3- ynoic acids and their use as reliable chiral derivatizing agents

Journal of Organic Chemistry

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Synthesis of acyldodecaheterocycles derived from (1R)-(-)-myrtenal and evaluation as chiral auxiliaries

Tetrahedron: Asymmetry

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Synthesis of acyldodecaheterocycles derived from (1R)-(-)-myrtenal and evaluation as chiral auxiliaries

Tetrahedron Asymmetry

journal-article

Derivatives of 10,16-dihydroxyhexadecanoic acid isolated from tomato (Solanum lycopersicum) as potential material for aliphatic polyesters

Molecules

journal-article

In vitro antifungal activity of coumarin extracted from Loeselia mexicana Brand

Mycoses

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Myrtenal, a controversial molecule for the proper application of the CIP sequence rule for multiple bonds

Natural Product Communications

journal-article

Synthesis of 6-bromo-2-arylindoles using 2-iodobenzoic acid as precursor

Tetrahedron Letters

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Absolute configuration of (-)-myrtenal by vibrational circular dichroism

Phytochemistry

journal-article

Efficient total synthesis of racemic bisabolane sesquiterpenes curcuphenol and xanthorrhizol starting from substituted acetophenones

Helvetica Chimica Acta

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Versatile synthesis of quaternary 1,3-oxazolidine-2,4-diones and their use in the preparation of α-hydroxyamides

Tetrahedron Letters

journal-article

A new synthetic route of 2-aroyl- and 2-benzyl-benzofurans and their application in the total synthesis of a metabolite isolated from dorstenia gigas

Australian Journal of Chemistry

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Genotoxic and cytotoxic effects produced by acetogenins obtained from Annona cherimolia Mill.

Biological and Pharmaceutical Bulletin

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New 2-acyl-1,3-dioxane derivatives from (1R)-(-)-myrtenal: stereochemical effect on their relative ability as chiral auxiliaries

Tetrahedron Asymmetry

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Synthesis of a New (1R)-(-)-Myrtenal Derived Dioxadithiadodecacycle and its Use as Efficient Chiral Auxiliary

Organic Letters

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Synthesis of a new (1R)-(-)-myrtenal-derived dioxadithiadodecacycle and its use as an efficient chiral auxiliary

Organic Letters

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Antifungal and antibacterial activity of four selected Mexican medicinal plants

Pharmaceutical Biology

journal-article

Enantioselective synthesis of either enantiomer of α-alkyl-α- hydroxy-α-phenylacetic acids using chiral auxiliaries

Tetrahedron Asymmetry

journal-article

Efficient and highly diastereoselective preparation of a myrtenal derived bis-sulfoxide and its preliminary evaluation as chiral acyl donor

Tetrahedron Letters

journal-article

Parallel and automated library synthesis of 2-long alkyl chain benzoazoles and azole[4,5-b]pyridines under microwave irradiation

Molecular Diversity

journal-article

Crankshaft motion in a highly congested bis(triarylmethyl)peroxide

Journal of the American Chemical Society

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Evaluation of corrosion inhibitors synthesized from fatty acids and fatty alcohols isolated from sugar cane wax

Corrosion

journal-article

Molecular Compasses and Gyroscopes: Engineering Molecular Crystals with Fast Internal Rotation

Crystal Growth and Design

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Molecular Crystals with Moving Parts: Synthesis, Characterization, and Crystal Packing of Molecular Gyroscopes with Methyl-Substituted Triptycyl Frames

Journal of Organic Chemistry

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New S,O-acetals from (1R)-(-)-myrtenal as chiral auxiliaries in nucleophilic additions

Tetrahedron Letters

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Antifungal activities of nine traditional Mexican medicinal plants

Journal of Ethnopharmacology

journal-article

Enantioselective synthesis of 1-alkyl-substituted 1-phenyl-1,2-ethanediols using a myrtenal-derived chiral auxiliary

Tetrahedron Asymmetry

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Synthesis of Long Chain 2-Alkyl-1-(2-hydroxyethyl)-2-imidazolines under Microwave in Solvent-Free Conditions

Synlett

journal-article

Effects of chlorophyllin on acetaldehyde: Lack of modulation of the rate of sister-chromatid exchanges in mouse bone marrow, and of complex formation in aqueous solution

Food and Chemical Toxicology

journal-article

Molecular compasses and gyroscopes. II. Synthesis and characterization of molecular rotors with axially substituted bis[2-(9-triptycyl)ethynyl]arenes

Journal of the American Chemical Society

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Use of the SOS-chromotest spot assay as a screening system for detecting genotoxic compounds in crude plant extracts

ATLA Alternatives to Laboratory Animals

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Generation of the new quirogane skeleton by a vinylogous retro-Michael type rearrangement of longipinene derivatives

Tetrahedron

journal-article

Highly diastereoselective nucleophilic additions using a novel myrtenal-derived oxathiane as a chiral auxiliary

Tetrahedron Asymmetry

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Regio- and stereoselectivity of captodative olefins in 1,3-dipolar cycloadditions. A DFT/HSAB theory rationale for the observed regiochemistry of nitrones

Journal of Organic Chemistry

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Steps to demarcate the effects of chromophore aggregation and planarization in poly(phenyleneethynylene)s. 2. The photophysics of 1,4-diethynyl-2-fluorobenzene in solution and in crystals

Journal of Organic Chemistry

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A new synthesis of peptidyl epoxysuccinates for probing cysteine protease-inhibitor P3/S3 binding interactions

Synthesis

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Phytochemical studies on Senna skinneri and Senna wislizeni

Natural Product Letters

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Knoevenagel condensation in heterogeneous phase catalyzed by IR radiation and Tonsil Actisil FF

Synthetic Communications

journal-article

Theoretical and experimental APT and DEPT behavior of methane

Spectroscopy Letters

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Structural, spectroscopic, and theoretical study of 1-acetylvinyl p-nitrobenzoate, a highly reactive and selective captodative olefin in cycloaddition reactions

Journal of Physical Chemistry A

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Highly selective 1,3-dipolar cycloadditions of captodative olefins 1-acetylvinyl carboxylates to diverse dipoles

Tetrahedron Letters

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Highly stereoselective palladium-catalyzed coupling reactions of captodative olefins acetylvinyl arenecarboxylates

Journal of Organometallic Chemistry

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Lewis acid-promoted stereoselective Diels-Alder cycloadditions of captodative olefins acetylvinyl carboxylates and NMR structural study of their cyclopentadiene adducts

Anales de Quimica

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Mechanistic studies of the longipinane to arteagane rearrangement

Journal of Natural Products

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Synthesis of acetamido(indol-3-yl)propanol derivatives

Heterocycles

journal-article

The chemical constituents of Rhamnus serrata var. Serrata

Natural Product Letters

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35Cl/37Cl one‐bond isotope effects on 13C chemical shifts in a series of para‐substituted chlorobenzenes

Magnetic Resonance in Chemistry

journal-article

Anthracenones and anthraquinones from roots of five species of the genus Karwinskia

Phytochemistry

journal-article

Knoevenagel condensation catalyzed by a Mexican bentonite using infrared irradiation

Synthetic Communications

journal-article

Molecular rearrangement of rastevione mesylate into arteagane derivatives

Journal of Natural Products

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Stereoselective synthesis, NMR conformational study and Diels-Alder reaction of β-functionalized 1-acetylvinyl arenecarboxylates

Tetrahedron

journal-article

Deuterium isotope effects as evidence for substituent perturbation of the π‐electron frame in benzanilides

Magnetic Resonance in Chemistry

journal-article

Highly efficient synthesis of the natural spiro-terpenoid (±)-andirolactone

Synthesis

journal-article

Novel heterocyclic outer-ring dienes: N-alkyland N-aryl substituted 4,5-dimethylene-2-oxazolidinones

Heterocycles

journal-article

Fischer indole synthesis of (β-Oxo)Indol-3-Yl Ketones using protected 1,3-Dicarbonyl compounds

Synthetic Communications

journal-article

Synthesis of 3,3-Dimethylenedithio-5-Oxyaldehydes

Synthetic Communications

journal-article

A PC program for calculation of dihedral angles from 1H NMR data

Tetrahedron Computer Methodology

journal-article

Synthese directe d'indoles anti-hypertensifs

Tetrahedron

journal-article

Synthèse brève de l'indorénate

Tetrahedron Letters

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